HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 54046793, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 54019979 | HCID 54019979 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 54046793 | HCID 54046793 | — |
Reaction Steps
Saturate with NH3 a solution of 6.7 g (20 mmole) N-methyl-N-[4-(hexafluoro-2-hydroxy-2-propyl)phenyl]carbamyl chloride in 200 ml Et2O. After 24 hours, wash the Et2O with water, then 1N HCl. Dry, concentrate and recrystallize the solid from ether-hexane to give 5.0 g white solid; m.p. 181°-184°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04093742 |
| Source dataset | uspto-grants-1978_06 |
| ORD ID | ord-0b268b092fe2432987414e65e58af06b |
| Source note | uspto-grants-1978_06 |