HRID839202

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID176

Acetic Acid

C2H4O2

HCID702

Ethanol

C2H6O

HCID7516

Phenylhydrazine

C6H8N2

HCID71394061

Methyl 2-[1-(5-nitrofuran-2-yl)ethylidene]hydrazine-1-carboxylate

C8H9N3O5

PRODUCTS

生成物

结构：O=Cc1cn(-c2ccccc2)nc1-c1ccc([N+](=O)[O-])o1

HCID20326255

3-(5-Nitrofuran-2-yl)-1-phenyl-1H-pyrazole-4-carbaldehyde

C14H9N3O4

PROCEDURE

实验过程

boiling 5-nitro-2-acetylfuran-methoxycarbonylhydrazone with 1.5 moles of phenylhydrazine and 0.1 mole of glacial acetic acid in ethanol for 3 hours under reflux.

WORKUP

后处理

customfor 3 hours
temperatureunder reflux