HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 54374358, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | N-{[1-Methyl-3-(5-nitrofuran-2-yl)-1H-pyrazol-4-yl]methylidene}hydroxylamine | HCID 54488696 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 54374358 | HCID 54374358 | 83% |
Reaction Steps
Stir together 2.5 g of 1-methyl-3-(5-nitro-2-furyl)pyrazole-4-carboxaldehydeoxime, 1.27 g of acetic anhydride and 10 ml of benzene for 2 hours at from 80° to 85° C. Cool the resulting solution and vacuum filter to obtain 1-methyl-3-(5-nitro-2-furyl)pyrazole-4-carboxaldehyde-(O-acetyloxime) [m.p. 192° to 197° C (with decomposition) from toluene] with a yield of 83%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04093812 |
| Source dataset | uspto-grants-1978_06 |
| ORD ID | ord-24d068d3ef884ed8ab982ebd90ebe890 |
| Source note | uspto-grants-1978_06 |