HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → 1-Methyl-5-(5-nitrofuran-2-yl)-1H-pyrazole-4-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 20326245 | HCID 20326245 | — |
| Product | 1-Methyl-5-(5-nitrofuran-2-yl)-1H-pyrazole-4-carbonitrile | HCID 20326063 | — |
Reaction Steps
Following the procedure of Example 21, react 1.3 g of 5-(2-furyl)-1-methylpyrazole-4-carbonitrile [German Offenlegungsschrift (DOS) 1,809,386] with 11.5 ml of acetic anhydride and 3 ml of 65% nitric acid to obtain 1-methyl-5-(5-nitro-2-furyl)pyrazole-4-carbonitrile [m.p. 149.5° to 151.5° C].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04093812 |
| Source dataset | uspto-grants-1978_06 |
| ORD ID | ord-2cca975e37f5410bbadde656edbdbd1d |
| Source note | uspto-grants-1978_06 |