HCID 20324274, compound → HCID 15328860, compound

Participants

Reaction Steps

0.6 g. of 10% palladium-on-carbon and added to a solution of 29 g. of 4-bromo-α-vinyl-benzhydrol in 300 ml. of benzene, and the mixture is hydrogenated at room temperature under atmospheric pressure. After the uptake of the calculated amount of hydrogen the catalyst is filtered off, and the benzene is evaporated from the clear filtrate under reduced pressure. 25 g. of clear, viscous oil, boiling at 140° C (0.8 mmHG.) are obtained as residue.

Provenance & Evidence