HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Dioxide → HCID 86735764, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Dioxide | HCID 280 | — |
| Reactant | Carbohydrazide | HCID 73948 | — |
| Reactant | 1-Butanesulfonyl chloride | HCID 75430 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86735764 | HCID 86735764 | — |
Reaction Steps
A mixture of 11.25 g (0.125 mole) carbohydrazide, 25 g sodium bicarbonate, 200 ml methanol and 37 g (0.25 mole) 1-butanesulfonyl chloride was heated to 60° C until evolution of CO2 ceased. The mix was cooled and water was added to precipitate the product. The initial precipitate weighed 12 g (dry). This melted with decomposition at 195°-197° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04096100 |
| Source dataset | uspto-grants-1978_06 |
| ORD ID | ord-1d2326a3e8174222bf77a5207ca102b0 |
| Source note | uspto-grants-1978_06 |