Methyl Salicylate → HCID 54403786, compound

Participants

Reaction Conditions

Reaction Steps

To a one liter, stainless steel autoclave was added 535 g. (3.52) of methyl salicylate (III) and 6.0 g. triethylamine. The resulting mixture was heated at 120° C, while 260 g. (4.5 moles) of propylene oxide was added over a one hour period. The reaction mixture was then heated up to 150° C and allowed to digest for 8 hr.

Provenance & Evidence