HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylhydrazine → 2-phenylphthalazin-1(2h)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylhydrazine | HCID 7516 | — |
| Reactant | 2-(dibromomethyl)benzoic acid | HCID 345553 | — |
| Product | 2-phenylphthalazin-1(2h)-one | HCID 235626 | 30.1% |
Reaction Steps
α,α-dibromo-o-toluic acid (29.4 g) and phenylhydrazine (34.6 g) were allowed to react as in Example 4. There was obtaoined 6.7 g (yield: 30%) of 2-phenyl-1-phthalazinone having a melting poin of 104°-105° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04096143 |
| Source dataset | uspto-grants-1978_06 |
| ORD ID | ord-08dba768ac024693b221cbd8dfac69ec |
| Source note | uspto-grants-1978_06 |