Hydrochloric Acid → HCID 20323303, compound

HRID 839506Notes

Reaction equation

HRID 839506 reaction equation
[CH2:1]1[CH:14]2[CH:5]([N:6]3[CH:11]([CH2:12][C:13]2=[O:15])[C:10]2[CH:16]=[CH:17][CH:18]=[CH:19][C:9]=2[CH2:8][CH2:7]3)[CH2:4][CH2:3][CH2:2]1.Cl>>[CH2:1]1[CH:14]2[CH:5]([N:6]3[CH:11]([CH2:12][CH:13]2[OH:15])[C:10]2[CH:16]=[CH:17][CH:18]=[CH:19][C:9]=2[CH2:8][CH2:7]3)[CH2:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 12774480HCID 12774480, compound

Product 1

HCID 20323303HCID 20323303, compound

Procedure

The following products are obtained when in Example 1 (A) appropriate amounts of the ketone derivatives listed below are substituted for 1,2,3,4,4a,6,7,11b,12,13a-decahydrodibenzo[a,f]quinolizin-13-one, the residual oil is additionally treated with excess ethereal hydrochloric acid and the precipitate is recrystallized from butanonemethanol.

Workup

  1. customthe precipitate is recrystallized from butanonemethanol

Sources & evidence

ORD record
ord-a5070a9b2b0e4727a863b27350e58f7e
Source dataset
uspto-grants-1978_06
Patent number
US04096147

Reaction notes

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