反应详情

温度

23 °C

A 50ml round-buttomed flask provided with a magnetic stirrer was charged with 10 mmol of benzaldehyde, 10 mmol of 2-chloro-3,3,4,4-tetramethylcyclobutanone, 12 mmol of sodium cyanide, 20 ml of a solvent and 1 ml of water. The reaction mixture was stirred vigorously at a temperature of 23° C. Two experiments ware carried out in this manner. Table II states the solvents used and presents the yields of the alpha-cyanobenzyl 2,2,3,3-tetramethylcyclopropanecarboxylate formed.

1. customA 50ml round-buttomed flask provided with a magnetic stirrer