Indacrinone → 76698-88-9

HRID 839707Notes

Reaction equation

HRID 839707 reaction equation
[O:1]=[C:2]1[C:10]2[C:5](=[CH:6][C:7]([O:13][CH2:14][C:15]([OH:17])=[O:16])=[C:8]([Cl:12])[C:9]=2[Cl:11])[CH2:4][C:3]1([CH3:24])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1.C(=O)(O)[O-].[Na+:29]>O>[O:1]=[C:2]1[C:10]2[C:5](=[CH:6][C:7]([O:13][CH2:14][C:15]([O-:17])=[O:16])=[C:8]([Cl:12])[C:9]=2[Cl:11])[CH2:4][C:3]1([CH3:24])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1.[Na+:29]

Participants

4

Reactant 2

HCID 42266IndacrinoneHCID 516892Sodium Bicarbonate

Product 1

HCID 8673578076698-88-9

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

(1-Oxo-2-methyl-2-phenyl-6,7-dichloro-5-indanyloxy)acetic acid (1 gm.) is treated with sodium bicarbonate (0.25 gm.) in water (10 ml.) and the mixture stirred and heated to effect solution. The solution is diluted with water to a volume of 50 ml. and sterilized by autoclaving at 120° C. for one hour.

Workup

  1. temperatureheated

Sources & evidence

ORD record
ord-43959bc1355d4ecba7c5c49f0feae7e2
Source dataset
uspto-grants-1978_06
Patent number
US04096267

Reaction notes

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