HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Ethanedithiol → 2,3-Dimercaptopropane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Ethanedithiol | HCID 33645 | — |
| Reactant | 3-Benzoylpropionic acid | HCID 72871 | — |
| Reactant | 2-Phenyl-1,3-dithiolane-2-propionic acid | HCID 54309792 | — |
| Product | 2,3-Dimercaptopropane | HCID 61217 | — |
| Product | 2,3-Butanedithiol | HCID 548353 | — |
Reaction Steps
In the same manner, 4-phenyl-4-oxobutyric acid is converted to 2-phenyl-1,3-dithiolane-2-propionic acid using ethanedithiol; while the use of 1,2-propanedithiol and 2,3-butanedithiol affords 4-methyl- and 4,5-dimethyl-2-phenyl-1,3-dithiolane-2-propionic acid, respectively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04096155 |
| Source dataset | uspto-grants-1978_06 |
| ORD ID | ord-eace0950a01d46e9bf84b497e39508fb |
| Source note | uspto-grants-1978_06 |