HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 86735785, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | N-Butyl-N-[(pyridin-2-yl)methyl]-2,5-bis(2,2,2-trifluoroethoxy)benzamide | HCID 20321976 | — |
| Product | HCID 86735785 | HCID 86735785 | — |
Reaction Steps
Using the method of Example 12 except omitting the treatment with sodium hydroxide, 4.64 g. of 2,5-bis(2,2,2-trifluoroethoxy)-N-n-butyl-N-(2-pyridylmethyl)benzamide is reduced to provide white solid product, 2,5-bis(2,2,2-trifluoroethoxy)-N-n-butyl-N-(2-piperidylmethyl)benzamide acetate, m.p. 119°-120° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04097481 |
| Source dataset | uspto-grants-1978_06 |
| ORD ID | ord-05fcbf3093984a8684b5fdcd504928aa |
| Source note | uspto-grants-1978_06 |