HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Acetate → Methyl 6-methoxymethyloxy-2-naphthyl-alpha-methylacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Acetate | HCID 6584 | — |
| Reactant | Chloromethyl Methyl Ether | HCID 7864 | — |
| Reactant | 2-(6-Hydroxy-naphthalen-2-yl)-propionic acid methyl ester | HCID 598897 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Methyl 6-methoxymethyloxy-2-naphthyl-alpha-methylacetate | HCID 21412543 | — |
Reaction Steps
A mixture of 23 g. of methyl 6-hydroxy-2naphthyl-α-methylacetate, methylacetate, 25 g. of chlorodimethyl ether, and 500 ml. of dimethylformamide is allowed to stand at room temperature for 12 hours. The reaction mixture is evaporated under reduced pressure to give methyl 6-methoxymethyloxy-2-naphthyl-α-methylacetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04097674 |
| Source dataset | uspto-grants-1978_06 |
| ORD ID | ord-cdff7ea19b474a98af5a7569e8abaf65 |
| Source note | uspto-grants-1978_06 |