HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 12474700, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Ethyl 2-octylcycloprop-2-ene-1-carboxylate | HCID 22621698 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 12474700 | HCID 12474700 | 81.5% |
Reaction Steps
Ethyl 2-octylcycloprop-2-ene-1-carboxylate (1.12 g, 5 mmol) and 100 ml of 0.2 N potassium hydroxide were stirred at room temperature for one week. Ether was added and the phases were separated. The aqueous phase was acidified and extracted with methylene chloride. The organic phase was dried over magnesium sulfate and stripped to give 0.8 g of 2-octylcycloprop-2-ene-1-carboxylic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06365549B2 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-cf19c3b1ee5b4fdeb74266067d37b03a |
| Source note | uspto-grants-2002_04 |