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HRID840126

反应详情

EQUATION

反应方程式

HRID 840126 的结构方程式

REACTANTS

反应物

3
结构：NCCCN1CCN(c2ccccc2OCC(F)(F)F)CC1
HCID10567490

4-[2-(2,2,2-Trifluoroethoxy)phenyl]-1-piperazinepropanamine

C15H22F3N3O

结构：O=C(O)c1conc1-c1ccc(F)cc1
HCID23447885

未命名化合物

结构：NCCCN1CCN(c2ccc(F)cc2OCC(F)(F)F)CC1
HCID23447911

未命名化合物

PRODUCTS

生成物

1
结构：O=C(NCCCN1CCN(c2ccccc2OCC(F)(F)F)CC1)c1conc1-c1ccccc1
HCID23447905

未命名化合物

收率 88%

PROCEDURE

实验过程

The title compound was prepared according to the procedure described in Example 8, but substituting compound 15B for Compound 8D and Compound 12B for Compound 8B. Purification by flash chromatography (ethyl acetate-2 N ammonia in methanol 95:5) yielded the title product (88%). M.p. 94.5-95.6° C.

WORKUP

后处理

  1. customThe title compound was prepared
  2. customPurification by flash chromatography (ethyl acetate-2 N ammonia in methanol 95:5)