1-Iodopropane → Butyl 6-[N-(5-bromo-2-propoxybenzyl)-N-ethylamino]pyridazine-3-carboxylate

HRID 840307Notes

Reaction equation

I[CH2:2][CH2:3][CH3:4].[Br:5][C:6]1[CH:7]=[CH:8][C:9]([OH:29])=[C:10]([CH:28]=1)[CH2:11][N:12]([C:15]1[N:20]=[N:19][C:18]([C:21]([O:23][CH2:24][CH2:25][CH2:26][CH3:27])=[O:22])=[CH:17][CH:16]=1)[CH2:13][CH3:14]>>[Br:5][C:6]1[CH:7]=[CH:8][C:9]([O:29][CH2:2][CH2:3][CH3:4])=[C:10]([CH:28]=1)[CH2:11][N:12]([C:15]1[N:20]=[N:19][C:18]([C:21]([O:23][CH2:24][CH2:25][CH2:26][CH3:27])=[O:22])=[CH:17][CH:16]=1)[CH2:13][CH3:14]

Participants

Reactant 2

HCID 336431-Iodopropane

HCID 22622486butyl 6-[N-(5-bromo-2-hydroxybenzyl)-N-ethylamino]pyridazine-3-carboxylate

Product 1

HCID 22622540Butyl 6-[N-(5-bromo-2-propoxybenzyl)-N-ethylamino]pyridazine-3-carboxylate

Procedure

The title compound was prepared by reacting 1-iodopropane and butyl 6-[N-(5-bromo-2-hydroxybenzyl)-N-ethylamino]pyridazine-3-carboxylate (reference example 3) using a similar method to that of reference example 4.

Sources & evidence

ORD record: ord-806b132421d04f8e90706eea37bf41ee
Source dataset: uspto-grants-2002_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06365603B1

Reaction notes

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