Bromomethylcyclopropane → HCID 22622495, compound
Reaction equation
[OH:1][C:2]1[CH:9]=[CH:8][C:7]([CH3:10])=[CH:6][C:3]=1[CH:4]=[S:5].Br[CH2:12][CH:13]1[CH2:15][CH2:14]1>>[CH:13]1([CH2:12][O:1][C:2]2[CH:9]=[CH:8][C:7]([CH3:10])=[CH:6][C:3]=2[CH:4]=[S:5])[CH2:15][CH2:14]1Participants
3
Procedure
2-Hydroxy-5-methylthiobenzaldehyde was alkylated with bromomethylcyclopropane using a similar method to that of reference example 4 to give 2-cyclopropylmethoxy-5-methylthiobenzaldehyde.
Sources & evidence
- ORD record
- ord-326f574ffa1e49d7800f332ac4d101a8
- Source dataset
- uspto-grants-2002_04
- Patent number
- US06365603B1
Reaction notes
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