Acetic Acid → HCID 22623287, compound

Participants

Reaction Steps

A mixture of 29.1 g of 4-chloro-2-fluoroaniline, 29.6 g of phthalic anhydride, and 150 ml of acetic acid was heated under reflux for 2 hours under stirring. After allowing the mixture to cool, the reaction mixture was poured into water, and the precipitated solid was collected by filtration. The resulting solid was washed with water and dried under reduced pressure to afford 50.9 g of the title compound.

Provenance & Evidence