HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67183523, compound → Ethyl 3-[4-(5-methylpyridin-2-yl)phenyl]propanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67183523 | HCID 67183523 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Ethyl 3-[4-(5-methylpyridin-2-yl)phenyl]propanoate | HCID 67182542 | — |
Reaction Steps
10% Palladium on charcoal (0.8 g) was added to a solution of the compound obtained from step b above (1.8 g) in tetrahydrofuran (15 mL) at room temperature, and hydrogen was supplied at 50 psi in a Paar apparatus for 4 hours. The reaction mixture was filtered through a celite pad and concentrated to afford the title compound (1.8 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08846910B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-d7cb2973bd8a4b6fb9554f0893717899 |
| Source note | uspto-grants-2014_09 |