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HRID840472

反应详情

EQUATION

反应方程式

HRID 840472 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)Oc1ccc(I)cc1
HCID141793

4-Iodophenyl acetate

C8H7IO2

结构：C#CC(O)c1cc2c(cc1C)C(C)(C)CCC2(C)C
HCID22361502

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)Oc1ccc(C#CC(O)c2cc3c(cc2C)C(C)(C)CCC3(C)C)cc1
HCID22619470

未命名化合物

收率 25%

PROCEDURE

实验过程

Following the basic procedure of Example 11(d), by reacting 1.28 g (5 mmol) of α-ethynyl-5,6,7,8-tetrahydro-3,5,5,8,8-pentamethyl-2-naphthalenemethanol with 1.44 g (5.5 mmol) of 4-iodophenyl acetate, 480 mg (25%) of the expected compound, with a melting point of 129°-130° C., were obtained.