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HRID840474

反应详情

EQUATION

反应方程式

HRID 840474 的结构方程式

REACTANTS

反应物

2
结构：CS(=O)c1ccc(Br)cc1
HCID3013958

1-Bromo-4-(methanesulfinyl)benzene

C7H7BrOS

结构：C#CC(O)c1ccc2c(c1)C(C)(C)CCC2(C)C
HCID11817362

未命名化合物

PRODUCTS

生成物

1
结构：CS(=O)c1ccc(C#CC(O)c2ccc3c(c2)C(C)(C)CCC3(C)C)cc1
HCID22619415

未命名化合物

PROCEDURE

实验过程

Following the basic procedure of Example 32, by reacting 1.21 g (5 mmol) of αethynyl-5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenemethanol with 1.1 g (5 mmol) of 4-bromophenylsulfinylmethane, 177 mg (9%) of the expected sulfoxide compound, with a melting point of 121°-122° C., were obtained.

WORKUP

后处理

  1. customwith a melting point of 121°-122° C., were obtained