HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-iodobenzoate → HCID 22619469, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-iodobenzoate | HCID 69273 | — |
| Reactant | HCID 22619460 | HCID 22619460 | — |
| Product | HCID 22619469 | HCID 22619469 | 57.1% |
Reaction Steps
Following the basic procedure of Example 11(d), by reacting 2 g (8.6 mmol) of α-ethynyl-4,4-dimethyl-7-thiochromanmethanol with 2.25 g (8.6 mmol) of methyl 4-iodobenzoate, 1.8 g (57%) of the expected ester was obtained in the form of an yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06368608B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-724795f5a0714f90b3def643a83e6f26 |
| Source note | uspto-grants-2002_04 |