Azobisisobutyronitrile → HCID 86757922, compound

Participants

Reaction Steps

3,3-dimethoxypropene of Chemical Formula 9 (0.3 mole), maleic anhydride (0.1 mole), AIBN (0.8 g) and tetrahydrofuran (42 g) were placed in a 100 ml flask and the mixture was reacted at 65° C. under nitrogen or argon atmosphere for 8 hours. After the polymerization was completed, the polymers were precipitated from ethyl ether. The polymer precipitate was dried in vacuo to obtain pure resin represented by following Chemical Formula 10:

Provenance & Evidence