Azobisisobutyronitrile → HCID 86757922, compound

HRID 840495Notes

Reaction equation

HRID 840495 reaction equation
[C:1]1(=[O:7])[O:6][C:4](=[O:5])[CH:3]=[CH:2]1.[CH3:8]C(N=NC(C#N)(C)C)(C#N)C>O1CCCC1>[CH3:8][O:5][CH:4]([O:6][CH3:1])[CH:3]=[CH2:2].[C:4]1(=[O:5])[O:6][C:1](=[O:7])[CH:2]=[CH:3]1

Participants

4

Reactant 2

HCID 6547AzobisisobutyronitrileHCID 7923Maleic Anhydride

Product 1

HCID 86757922HCID 86757922, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

3,3-dimethoxypropene of Chemical Formula 9 (0.3 mole), maleic anhydride (0.1 mole), AIBN (0.8 g) and tetrahydrofuran (42 g) were placed in a 100 ml flask and the mixture was reacted at 65° C. under nitrogen or argon atmosphere for 8 hours. After the polymerization was completed, the polymers were precipitated from ethyl ether. The polymer precipitate was dried in vacuo to obtain pure resin represented by following Chemical Formula 10:

Workup

  1. customthe mixture was reacted at 65° C. under nitrogen
  2. customthe polymers were precipitated from ethyl ether
  3. customThe polymer precipitate was dried in vacuo
  4. customto obtain pure resin

Sources & evidence

ORD record
ord-92f36c56420f4dcd908e80e244f0b30f
Source dataset
uspto-grants-2002_04
Patent number
US06368773B1

Reaction notes

Loading…