HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Aminomethyl)aniline → HCID 66158495, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Aminomethyl)aniline | HCID 178096 | — |
| Reactant | 5-Methylisoxazole-3-carbonyl chloride | HCID 2736894 | — |
| Product | HCID 66158495 | HCID 66158495 | — |
Reaction Steps
2-Aminobenzylamine (490 mg, 4.01 mmol) and 5-methyl-3-isoxazoyl chloride (437 mg, 3.01 mmol) were converted to the title compound by the procedure of Preparation 1 to yield 250 mg. (36%). MS(FD) m/z 231 (M+). 1H NMR consistent with desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06369070B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-c571d24560a4434e8bec82484dab27c4 |
| Source note | uspto-grants-2002_04 |