HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 4-(4-Chlorophenoxy)-3-nitroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 4-Chlorophenol | HCID 4684 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Fluoro-3-nitroaniline | HCID 67768 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 4-(4-Chlorophenoxy)-3-nitroaniline | HCID 15580149 | — |
Reaction Steps
1.4 g of potassium carbonate were added to a solution of 1.29 g of 4-chlorophenol in 8 ml of DMF and, after stirring for 30 minutes, 1.6 g of 4-fluoro-3-nitroaniline were added, and the mixture was stirred at 100° C. for 3 hours. After cooling, 80 ml of water were added and, after brief stirring, the precipitate was filtered off with suction and dried in vacuo at 40° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06369088B2 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-2d2d4a3caa8e4672b35ef0db46ad0d4c |
| Source note | uspto-grants-2002_04 |