HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 69968776, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 22620261 | HCID 22620261 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 69968776 | HCID 69968776 | — |
Reaction Steps
The latter compound was prepared by reacting 5-methoxy-3-(4-(4-chlorobutanoylamino)-3-methylphenyl)-3H-(1,3,4)oxadiazol-2-one with sodium hydride in dioxane at room temperature and purifying the crude product by column chromatography (silica gel, methylene chloride:methanol=98:2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06369088B2 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-51ec78ecbb92488d8afbe14bfd035df1 |
| Source note | uspto-grants-2002_04 |