HuagongsheHuagongshe Chemistry Print Report · For research reference only
trans-2-Phenyl-1-cyclopropanecarbonyl chloride → HCID 86588256, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | trans-2-Phenyl-1-cyclopropanecarbonyl chloride | HCID 13656 | — |
| Reactant | HCID 178507432 | HCID 178507432 | — |
| Product | HCID 86588256 | HCID 86588256 | — |
Reaction Steps
Bis-trans-2-phenyl-cyclopropanecarbonyl benzimidazole was prepared by method C from 2-(4-aminophenyl)-6-amino-benzimidazole (0.500 g, 2.23 mmole) and trans-2-phenyl-1-cyclopropanecarbonyl chloride (0.831 ml, 0.966 g, 5.35 mmole). The resulting solid was purified on silica gel (5% MeOH in CH2Cl2). HPLC showed the product was 95.5% pure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06369091B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-2a1de0775e5a48f789d1ce18751fcaec |
| Source note | uspto-grants-2002_04 |