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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 840743Generated: October 31, 2026

Oxalyl chloride → HCID 178444536, compound

https://huagongshe.com/reaction/840743

Reaction equation

Participants

RoleNameHCIDCharge
ReactantOxalyl chlorideHCID 65578—
ReactantHCID 178444557HCID 178444557—
ReactantHCID 178507432HCID 178507432—
CatalystDimethylformamideHCID 6228—
SolventPyridineHCID 1049—
ProductHCID 178444536HCID 178444536—

Reaction Steps

Bis-trans-4-pentylcyclohexyl carbonyl benzimidazole was synthesized as follows: oxalyl chloride (1.07 ml, 2 M in CH2Cl2) was added to trans-4-pentylcyclohexyl carboxylic acid (0.424 g, 2.14 mmole) followed by one drop DMF. The mixture was allowed react at RT for 1 hour. To the above solution was added 2-(4-aminophenyl)-6-amino-benzimidazole (0.200 g, 0.89 mmole) in pyridine (2 ml). The

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06369091B1
Source datasetuspto-grants-2002_04
ORD IDord-af425a41012c4e28bec7720c521208cc
Source noteuspto-grants-2002_04