HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 178444536, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 178444557 | HCID 178444557 | — |
| Reactant | HCID 178507432 | HCID 178507432 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 178444536 | HCID 178444536 | — |
Reaction Steps
Bis-trans-4-pentylcyclohexyl carbonyl benzimidazole was synthesized as follows: oxalyl chloride (1.07 ml, 2 M in CH2Cl2) was added to trans-4-pentylcyclohexyl carboxylic acid (0.424 g, 2.14 mmole) followed by one drop DMF. The mixture was allowed react at RT for 1 hour. To the above solution was added 2-(4-aminophenyl)-6-amino-benzimidazole (0.200 g, 0.89 mmole) in pyridine (2 ml). The
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06369091B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-af425a41012c4e28bec7720c521208cc |
| Source note | uspto-grants-2002_04 |