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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 840787Generated: October 30, 2026

Hydrochloric Acid → HCID 178472622, compound

https://huagongshe.com/reaction/840787

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 178472629HCID 178472629—
CatalystPalladium hydroxideHCID 9942167—
SolventEthanolHCID 702—
ProductHCID 178472622HCID 178472622—

Reaction Steps

A solution of the compound of Example 9 (0.43 mmol) in absolute ethanol (10 mL) was treated with Pd(OH)2 (46 mg, 0.086 mmol) and concentrated HCl (1 mL). The mixture was hydrogenated in a PARR shaker at 40 p.s.i. for 5 h. The mixture was filtered through Celite to remove the catalyst and the filtrate was evaporated under reduced pressure to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06369063B1
Source datasetuspto-grants-2002_04
ORD IDord-3abea8241ca8433dace354d5835260fe
Source noteuspto-grants-2002_04