HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70091156, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 70091218 | HCID 70091218 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70091156 | HCID 70091156 | 167.1% |
Reaction Steps
A solution of the compound of Example 29 (1 g, 2.4 mmol) in absolute ethanol (10 mL) was treated with 5%Pd/C (200 mg) and concentrated HCl (2 mL). The mixture was hydrogenated at 40 p.s.i. for 2 hours. The mixture was filtered through Celite to remove the catalyst and the filtrate was evaporated under reduced pressure to give the title compound (1.1 g, 81% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06369063B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-b49854927d534308816012e78fa944b0 |
| Source note | uspto-grants-2002_04 |