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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 840792Generated: October 30, 2026

Hydrochloric Acid → HCID 70091156, compound

https://huagongshe.com/reaction/840792

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 70091218HCID 70091218—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 70091156HCID 70091156167.1%

Reaction Steps

A solution of the compound of Example 29 (1 g, 2.4 mmol) in absolute ethanol (10 mL) was treated with 5%Pd/C (200 mg) and concentrated HCl (2 mL). The mixture was hydrogenated at 40 p.s.i. for 2 hours. The mixture was filtered through Celite to remove the catalyst and the filtrate was evaporated under reduced pressure to give the title compound (1.1 g, 81% yield).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06369063B1
Source datasetuspto-grants-2002_04
ORD IDord-b49854927d534308816012e78fa944b0
Source noteuspto-grants-2002_04