HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-[(methylsulfonyl)methyl]aniline(SALTDATA: FREE) → HCID 178504867, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-[(methylsulfonyl)methyl]aniline(SALTDATA: FREE) | HCID 12843964 | — |
| Reactant | 8-[Ethoxymethylidene]-6H-[1,3]thiazolo[5,4-e]indol-7-one | HCID 53990807 | — |
| Product | HCID 178504867 | HCID 178504867 | 66% |
Reaction Steps
The title compound was prepared in 66% yield from 8-ethoxymethylene-6,8-dihydro-1-thia-3,6-diaza-as-indacen-7-one and 4-methylsulfonylmethylaniline according to Procedure J: 1H NMR (DMSO-d6): δ11.1 (d, 1H), 11.0 (s, 1H), 9.3 (s, 1H), 8.1 (d, 1H), 7.8 (d, 1H), 7.5 (q, 4H), 7.1 (d, 1H), 4.45 (s, 2H), 2.9 (s. 3H); APCI−MS m/z 384 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06369086B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-3ed5f4027bff46e0b6cfcceb6367ea9b |
| Source note | uspto-grants-2002_04 |