HuagongsheHuagongshe Chemistry Print Report · For research reference only
20633-28-7 → HCID 22620527, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 20633-28-7 | HCID 22620478 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 22620527 | HCID 22620527 | 89.2% |
Reaction Steps
3,3-Dimethyl-5-oxo-5-phenylpentanoic acid (17.0 g, 77.2 mmol) was subjected to hydrogen catalytic reduction in acetic acid (170 ml) by using 10% palladium-carbon as a catalyst. After completion of the reaction, the catalyst was filtered off and the solvent was distilled off under reduced pressure to obtain 14.2 g of 3,3-dimethyl-5-phenylpentanoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06369110B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-4f9a39995b6f4a988c7badb1a328a8f8 |
| Source note | uspto-grants-2002_04 |