Anisole → HCID 18400084, compound

Participants

Reaction Steps

1.5 g of 3′-chloro-4′-(4-chloro-5-formyl-2-phenylimidazol-1-ylmethyl)biphenyl-2-sulfonic acid tert-butylamide and 340 μl of anisole are dissolved in 10 ml of trifluoroacetic acid and stirred at RT for 24 h. The volatile constituents are removed in vacuo, the residue is taken up twice with 50 ml of toluene each time and the volatile constituents are again removed in vacuo. 1.5 g of a colorless foam are obtained.

Provenance & Evidence