HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 22620843, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 22620849 | HCID 22620849 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22620843 | HCID 22620843 | — |
Reaction Steps
A solution of sodium borohydride in methanol was cooled to 5° C. A solution of 4-oxo-pentanoic acid {4-[4-(4-oxo-pentanoylamino)-benzenesulfonyl]-phenyl}-amide in THF was added and the resulting reaction mixture was stirred at room temperature. After workup and purification, the product was obtained as a colourless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06369248B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-52a2fe678352490b8f96060ced020a95 |
| Source note | uspto-grants-2002_04 |