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HRID84143

反应详情

EQUATION

反应方程式

HRID 84143 的结构方程式

REACTANTS

反应物

4
结构：ClC(Cl)Cl
HCID6212

Chloroform

CHCl3

结构：CCNCC
HCID8021

Diethylamine

C4H11N

结构：CCN1c2ccccc2C(CS(=O)(=O)Cl)=CC1(C)C
HCID12138182

未命名化合物

结构：CCN1c2ccccc2C(CS(=O)(=O)N2CCC(C(=O)OC)CC2)=CC1(C)C
HCID12138183

未命名化合物

PRODUCTS

生成物

1
结构：CCN1c2ccccc2C(CS(=O)(=O)N(CC)CC)=CC1(C)C
HCID12138187

未命名化合物

收率 79%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

N,N-diethyl-(1-ethyl-2,2-dimethyl-1,2-dihydroquinol-4-yl)-methanesulfon-amide (11) is prepared similarly to compound (10) using compound (9) with diethylamine. The product is isolated by column chromatography on silica gel with a gradient running from chloroform to ethanol.

WORKUP

后处理

  1. customThe product is isolated by column chromatography on silica gel with a gradient