HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 22618277, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 9944208 | HCID 9944208 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 22618277 | HCID 22618277 | — |
Reaction Steps
A solution of 2-(2-chlorobenzyl)-7-(3-hydroxy-1-propyl)benzoxazole (10 g, 0.033 mole) in ether (50 ml) was treated with methanesulfonyl chloride (4.4 g, 0.037 mol) and triethylamine 3.7 g, 0.037 mol). After stirring for 1 hour, the triethylamine hydrochloride was filtered and the ether was evaporated to give the title compound which was pure by TLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06372770B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-c539ac5faece419293130ac31efb272b |
| Source note | uspto-grants-2002_04 |