1-Bromooctane → HCID 22618805, compound

HRID 842278Notes

Reaction equation

HRID 842278 reaction equation
C([O:4][CH2:5][C:6]([NH:17]C(=O)C)([CH3:16])[CH2:7][CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([OH:15])[CH:10]=1)(=O)C.[CH2:21](Br)[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH3:28].[ClH:30].NC(CCC1C=CC=CC=1OCCCCCCC)(CCC)CO>>[ClH:30].[NH2:17][C:6]([CH3:16])([CH2:7][CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([O:15][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH3:28])[CH:10]=1)[CH2:5][OH:4]

Participants

4

Reactant 3

HCID 81401-BromooctaneHCID 22618715HCID 22618715, compoundHCID 54024837HCID 54024837, compound

Product 1

HCID 22618805HCID 22618805, compound

Procedure

2-Acetamido-4-(3-hydroxyphenyl)-2-methylbutyl acetate and octyl bromide were used in the same manner as working example 52 (9) and (10) to give the subject compound as white crystals, melting at 130-132° C.

Sources & evidence

ORD record
ord-5e1208c0fb2e4d10967aa1daa5958d92
Source dataset
uspto-grants-2002_04
Patent number
US06372800B1

Reaction notes

Loading…