HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → HCID 11323077, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | (R)-4-Benzyl-2-oxazolidinone | HCID 2734969 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 11323077 | HCID 11323077 | — |
Reaction Steps
reacting said (1R,6R)-6-methyl-3-cyclohexene-1-carboxylic acid (5) with I2, KI and NaHCO3 in methylene chloride to produce (1R,2R,4S,5s)4-iodo-2-methyl-6-oxabicyclo[3.2.1]octan-7-one (8),
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06375943B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-f0992252fc17439da4585191e6a1b795 |
| Source note | uspto-grants-2002_04 |