HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 11404582, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 2-(dimethylamino)-4-(trifluoromethyl)-6H-1,3-oxazin-6-one | HCID 3723862 | — |
| Reactant | HCID 11816030 | HCID 11816030 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 11404582 | HCID 11404582 | 57.3% |
Reaction Steps
A mixture of 0.2 g 1A, 0.268 g 2-dimethylamino-4-trifluoromethyl-1,3-oxazin-6-one (obtained according to M.-A. Decock-Plancquaert et al., Bull. Soc. Chim. Belg. 101 (4) 313-321 (1992)) and 10 ml acetic acid is refluxed for 4 hours. The mixture is poured into water, extracted and chromatographed to yield 0.23 g of 1B as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06376426B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-85098c0d155b4819aa2813af14cfe560 |
| Source note | uspto-grants-2002_04 |