HCID 22614804, compound → HCID 22614829, compound

Participants

Reaction Steps

The product from Example 11A and the product from Example 8D were processed as described in Example 1L to provide the title compound. mp 198-201° C.; [α]23D−7.8 °(c 1.02, DMSO); 1H NMR (300 MHz, DMSO-d6) δ1.60-1.85 (m, 4H), 2.80-3.75 (m, 7H), 3.78 (s,3H), 3.82-4.75 (m, 6H), 6.42-6.95 (m, 3H), 9.02 (s, 1H), 10.60 (bs, 1H), 1290 (s, 1H); MS (DCI/NH3) m/e 529 (M+H)+; Anal. calcd for C24H25N6O4SCl.2.0 HCl: C, 47.89; H, 4.52; N, 13.96. Found: C, 47.64; H, 4.62; N, 13.63.

Provenance & Evidence