HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydrosulfide → HCID 178508658, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydrosulfide | HCID 28015 | — |
| Reactant | 9-Benzyl-8-bromoadenine | HCID 9904551 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178508658 | HCID 178508658 | 99% |
Reaction Steps
910 mg (3.0 mmol) of 8-bromo-9-benzyladenine and 1.08 g of sodium hydrosulfide were added to 50 ml of ethanol and heated for 12 hr under refluxing. After the solvent was removed by distillation, the reaction product was dissolved in distilled water and neutralized with 1 N hydrochloric acid. Deposited crystals were collected by filtration to thereby obtain the captioned compound (770 mg; yield: 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06376501B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-b9fd250d3ceb4489b9c275bd3a1a07ee |
| Source note | uspto-grants-2002_04 |