HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 131723192, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Cyclohexanol, 3,3-dimethyl- | HCID 79105 | — |
| Reactant | 4-Nitrophenyl chloroformate | HCID 82129 | — |
| Product | HCID 131723192 | HCID 131723192 | — |
Reaction Steps
The product from Example 5, Step 1 was prepared as described above in Example 3, Step 1 starting with 3,3-dimethyl cyclohexanol (1.07 mmol), 4-nitrophenyl chloroformate (1.18 mmol) and pyridine (1.18 mmol).1H-NMR (CDCl3): 8.3 (d, 2H); 7.4 (d, 2H); 4.85 (m, 1H); 2.1 (m, 1H); 1.1-1.8 (m, 7H); 1.05 (s, 3H); 0.95 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06376496B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-0ef7463501fa45ee858603af793f3e22 |
| Source note | uspto-grants-2002_04 |