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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 842728Generated: October 31, 2026

Pyridine → HCID 131723192, compound

https://huagongshe.com/reaction/842728

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPyridineHCID 1049—
ReactantCyclohexanol, 3,3-dimethyl-HCID 79105—
Reactant4-Nitrophenyl chloroformateHCID 82129—
ProductHCID 131723192HCID 131723192—

Reaction Steps

The product from Example 5, Step 1 was prepared as described above in Example 3, Step 1 starting with 3,3-dimethyl cyclohexanol (1.07 mmol), 4-nitrophenyl chloroformate (1.18 mmol) and pyridine (1.18 mmol).1H-NMR (CDCl3): 8.3 (d, 2H); 7.4 (d, 2H); 4.85 (m, 1H); 2.1 (m, 1H); 1.1-1.8 (m, 7H); 1.05 (s, 3H); 0.95 (s, 3H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06376496B1
Source datasetuspto-grants-2002_04
ORD IDord-0ef7463501fa45ee858603af793f3e22
Source noteuspto-grants-2002_04