HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 14774175, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-Aminobenzonitrile | HCID 16702 | — |
| Reactant | HCID 14774174 | HCID 14774174 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 14774175 | HCID 14774175 | — |
Reaction Steps
A solution of 3-aminobenzonitrile (10 mmol) in 50 ml of chloroform and triethylamine (11 mmol) is added to a solution of 10 mmol of 3-(2-quinolinylmethyloxy)benzoic acid chloride in 20 ml of chloroform over a period of 10 minutes. The reaction is stirred at room temperature for 2 hours and is poured into water and then extracted into chloroform. The organic solution is dried and evaporated to give 3-(3-(2-quinolinylmethyloxy)benzoylamino)benzonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06376512B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-82a6213f76cb4ac5a3199646e7802cf6 |
| Source note | uspto-grants-2002_04 |