3-Methoxypropylamine → HCID 5153298, compound

HRID 843488Notes

Reaction equation

HRID 843488 reaction equation
F[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1.[CH3:11][O:12][CH2:13][CH2:14][CH2:15][NH2:16]>>[CH3:11][O:12][CH2:13][CH2:14][CH2:15][NH:16][C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 16723-MethoxypropylamineHCID 9590p-Fluoronitrobenzene

Product 1

HCID 5153298HCID 5153298, compound

Procedure

1-Fluoro-4-nitrobenzene (10 g, 70.8 mmoles) is refluxed for 5 hours with 36.5 g (410 mmoles) of 3-methoxy-propylamine. After that, the reaction product is poured onto 400 g of ice/water and the dye obtained is filtered off. A yellow dye with a melting point of 57°-59° C. is obtained.

Workup

  1. customthe dye obtained
  2. filtrationis filtered off
  3. customA yellow dye with a melting point of 57°-59° C. is obtained

Sources & evidence

ORD record
ord-0bce630aac72497f81ee43aa257f214d
Source dataset
uspto-grants-2002_04
Patent number
US06379400B1

Reaction notes

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