HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxypropylamine → HCID 5153298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxypropylamine | HCID 1672 | — |
| Reactant | p-Fluoronitrobenzene | HCID 9590 | — |
| Product | HCID 5153298 | HCID 5153298 | — |
Reaction Steps
1-Fluoro-4-nitrobenzene (10 g, 70.8 mmoles) is refluxed for 5 hours with 36.5 g (410 mmoles) of 3-methoxy-propylamine. After that, the reaction product is poured onto 400 g of ice/water and the dye obtained is filtered off. A yellow dye with a melting point of 57°-59° C. is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06379400B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-0bce630aac72497f81ee43aa257f214d |
| Source note | uspto-grants-2002_04 |