HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Fluoronitrobenzene → HCID 14495277, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Fluoronitrobenzene | HCID 9590 | — |
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Product | HCID 14495277 | HCID 14495277 | — |
Reaction Steps
1-Fluoro-4-nitrobenzene (3.5 g, 24.8 mmoles) is refluxed for 5 hours with 8.1 g (0.14 moles) of cyclopropylamine. After that, the reaction product is poured onto 250 g of ice/water and the precipitate is filtered off. After recrystallization from ethanol, a yellow solid with a melting point of 126°-128° C. is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06379400B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-7f76bc0ac8c84db88d768302fccc7b9e |
| Source note | uspto-grants-2002_04 |