HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-fluoro-2-methyl-4-nitro- → HCID 15789288, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-fluoro-2-methyl-4-nitro- | HCID 68001 | — |
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Product | HCID 15789288 | HCID 15789288 | — |
Reaction Steps
1-Fluoro-2-methyl-4-nitrobenzene (3.7 g, 24.8 mmoles) is refluxed for 5 hours with 8.1 g (0.14 moles) of cyclopropylamine. After that, the reaction product is poured onto 250 g of ice/water and the solid obtained is recrystallized from ethanol. A yellow solid with a melting point of 35°-37° C. is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06379400B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-ba31133c86f34f85b5c9f83a15e69919 |
| Source note | uspto-grants-2002_04 |