HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dodecylamine → dodecylsulfam
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dodecylamine | HCID 13583 | — |
| Reactant | Chlorosulfonic acid | HCID 24638 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | dodecylsulfam | HCID 204302 | — |
Reaction Steps
Dodecyl amine (0.1 mol) is added to a round bottom flask equipped with magnetic stirrer and dissolved in anhydrous pyridine. Next, chlorosulfonic acid (0.1 mol) is added dropwise with stirring to the chilled solution. The resulting product, dodecyl sulfamic acid, is then collected by filtration, washed with water and dried in an oven.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06380182B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-a4506359bda14e6486864383343f1663 |
| Source note | uspto-grants-2002_04 |